Synthesis and characterization of polyaniline/graphite conducting nanocomposites

A new method for the synthesis of exfoliated graphite and polyaniline (PANI)/graphite nanocomposites was developed. Exfoliated graphite nanosheets were prepared through the microwave irradiation and sonication of synthesized expandable graphite. The nanocomposites were fabricated via the in situ polymerization of the monomer at the presence of graphite nanosheets. The as-synthesized graphite nanosheets and PANI/graphite nanocomposite materials were characterized with Fourier transform infrared spectroscopy, scanning electron microscopy, transmission electron microscopy, and thermogravimetric analysis (TGA). The conductivity of the PANI/graphite nanocomposites was dramatically increased over that of pure PANI. TGA indicated that the incorporation of graphite greatly improved the thermal stability of PANI. © 2004 Wiley Periodicals, Inc. J Polym Sci Part B: Polym Phys 42: 1972–1978, 2004     

Microwave-assisted extraction of quercetin and acid degradation of its glycosides in Psidium guajava leaves.

Microwave-assisted extraction (MAE) and microwave-assisted hydrolysis (MAAH) were developed for the sample preparation of guava leaves prior to GC determination of quercetin and its glycosides. Ethanol was selected as the solvent. The optimum MAE temperature, particle size, solvent volume and MAE time are 120 degrees C, 40 - 60 mesh, 20 mL and 5 min, respectively; the optimum MAAH temperature and time, HCl concentration, solvent are 100 degrees C, 5 min, 1.2 mol L(-1) HCl and ethanol, respectively.     

A Kind of Electrode Enhanced the Electrochemiluminescence

Electrochemiluminescence (ECL), like other chemiluminescence technique, offers high signal-to-noise ratio. Furthermore, it has the advantage over other chemiluminescence techniques of being initiated by a voltage potential. Thus, it provides a better-controlled luminescence. This technique has been used in measuring many kinds of organic and inorganic matters, and analyzing many kinds of antigen, antibody and hapten, such as carcinoembryonic antigen and alpha-fetoprotein, etc1-6. The ele…     

Bounded Positive Solutions of Schrödinger Equations in Two-Dimensional Exterior Domains

We prove under quite general assumptions the existence of a bounded positive solution to the semilinear Schrödinger equation in a two-dimensional exterior domain.     

一类逆半群的亚直可约性

本文利用逆半群上的同余扩张，讨论了一类逆半群的亚直可约性，并刻划了这类逆半群的幂等元集的特征。     

高功率激光驱动器中小尺度自聚焦和噪声模型

 建立了一套线性的近似分析方法，研究高功率激光驱动器中强激光传输的小尺度自聚焦效应和相位噪声对光束传输和光束质量的影响，给出了系统噪声强度、B积分值与光束近场调制对比度之间的定量关系。研究表明,为保证输出光束质量，即近场调制对比度小于给定值，系统内的噪声强度必须符合一定的谱分布。     

基于虚拟仪器的人体皮肤组织吸收光谱检测平台

本文运用光电无损检测技术,采用皮外反射式测量方法,通过光纤光谱仪和虚拟仪器构建人体皮肤组织吸收光谱检测平台.该平台适合于光子-组织相互作用基础研究及激光美容临床检测,可协助医师进行病理诊断和病变程度判别.文中给出几个吸收光谱的检测结果.     

Generalized exponents of primitive simple graphs

The exponent of a primitive digraph has been generalized in [2]. In this paper we obtain new parameters on generalized exponent of primitive simple graphs (symmetric primitive (0,1) matrices with zero trace) completely.     

Magnetotunneling spectroscopy of a biased triple-barrier semiconductor heterostructure

In this work we describe a magnetotunneling spectroscopy technique for probing the localization degree of two-dimensional states and mapping the subbands in the active region of a resonant-tunneling semiconductor heterostructure. The reported experimental data consist of the low-temperature tunneling current traces of an asymmetric triple-barrier structure measured by sweeping an in-plane magnetic field up to 10 T. According to our interpretation model, the main features observed in the tunnel current traces are due to the field-induced resonant transitions between two-dimensional states at the crossing region between dispersion curves. The data reveals the highly localized nature of the quantum states in an asymmetric double-quantum-well structure even for those with very narrow middle barriers.